1,2,3,4-四氢-1-萘胺合成路线 （共 44 条）
反应条件
dihydrogen peroxide; poly(N-isopropylacrylamide) based tungsten catalyst in toluene T=60°C;
参考文献
Hamamoto, Hiromi; Suzuki, Yachiyo; Takahashi, Hideyo; Ikegami, Shiro
Tetrahedron Letters, 2007 , vol. 48, # 24 p. 4239 - 4242
反应条件
pyridoxal 5'-phosphate; recombinant ω-transaminase from Burkholderia vietnamiensis G4 in aq. buffer T=37°C; pH=7.4; 12 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Jiang, Jinju; Chen, Xi; Feng, Jinhui; Wu, Qiaqing; Zhu, Dunming
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 100, p. 32 - 39
参考文献
Bamberger; Bammann
Chemische Berichte, 1889 , vol. 22, p. 964
反应条件
pyridoxal 5'-phosphate; recombinant ω-transaminase from Burkholderia vietnamiensis G4 in aq. buffer T=37°C; pH=7.4; 12 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 100, p. 32 - 39
反应条件
hydrogenchloride; (+)-ketopinic acid; water; lithium diisopropyl amide Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron: Asymmetry, , vol. 5, # 5 p. 817 - 820
反应条件
coated protease in 3-methyl pentan-3-ol T=21°C; 456 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 9 p. 1759 - 1764
反应条件
N,N'-dimethyl-N,N'-propyleneurea T=-20°C; 24 h; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 25 p. 3314 - 3317
反应条件
Novozym 435 T=23°C; 2 h; Molecular sieveEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 23, # 3-4 p. 230 - 236
反应条件
hydrogenchloride; (+)-ketopinic acid; water; lithium diisopropyl amide Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM; ARMSTRONG, Daniel, W.; PING, Sun; BREITBACH, Zachary, S.; WANG, Chunlei
Patent: WO2010/148191 A2, 2010 ;
Location in patent: Page/Page column 45-50 ;
反应条件
Candida antarctica lipase B in n-heptane T=80°C; 26 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 18 p. 6918 - 6923
