(S)-(-)-1-苯基-1-丁醇合成路线 （共 63 条）
参考文献
Journal of Biological Chemistry, , vol. 97, p. 379,381
Journal of the Chemical Society, , p. 128
Journal of the American Chemical Society, , vol. 77, p. 1590,1591, 1593
反应条件
1: Et3N 2: H2, quinoline / Pd/BaSO4 4: H2 / Pd/C 5: 1.) BF3*2AcOH, 2.) MCPBA, Et3N View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 18 p. 1456 - 1457
反应条件
1: 56 percent / alumina / 24 h / Heating 2: 89 percent / imidazole / dimethylformamide / 3 h / 20 °C 3: 86 percent / LiAlH4 / diethyl ether / 1 h / 20 °C 4: 52 percent / pyridine; DMAP / 2 h / 20 °C 5: 92 percent / LiAlH4 / diethyl ether / 1 h / 20 °C 6: AcOH; H2O / tetrahydrofuran / 24 h / 40 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 12 p. 1685 - 1694
反应条件
1: 89 percent / imidazole / dimethylformamide / 3 h / 20 °C 2: 86 percent / LiAlH4 / diethyl ether / 1 h / 20 °C 3: 52 percent / pyridine; DMAP / 2 h / 20 °C 4: 92 percent / LiAlH4 / diethyl ether / 1 h / 20 °C 5: AcOH; H2O / tetrahydrofuran / 24 h / 40 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 12 p. 1685 - 1694
反应条件
1: H2 / Pd/C 2: 1.) BF3*2AcOH, 2.) MCPBA, Et3N View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 18 p. 1456 - 1457
反应条件
1: H2, quinoline / Pd/BaSO4 3: H2 / Pd/C 4: 1.) BF3*2AcOH, 2.) MCPBA, Et3N View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 18 p. 1456 - 1457
反应条件
1: Ph3P 2: H2 / Pd/C 3: 1.) BF3*2AcOH, 2.) MCPBA, Et3N View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 18 p. 1456 - 1457
反应条件
1: H2, quinoline / Pd/BaSO4 2: Ph3P 3: H2 / Pd/C 4: 1.) BF3*2AcOH, 2.) MCPBA, Et3N View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 18 p. 1456 - 1457
反应条件
2: H2 / Pd/C 3: 1.) BF3*2AcOH, 2.) MCPBA, Et3N View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 18 p. 1456 - 1457
反应条件
1: 1.) boron trifluoride 2.) aq. sodium hydrogen carbonate / 1.) AcOH, CH2Cl2, 20 deg C, 1.5 h 2.) 15 min 2: Et3N, m-chloroperbenzoic acid / diethyl ether / 20 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 24 p. 3331 - 3350
