[(1S)-1-(4-甲氧基苯基)乙基]氨基甲酸叔丁酯合成路线 （共 9 条）
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile T=0°C; 0.5 h; Yield given;
参考文献
Kim, Bong Jin; Park, Yong Sun; Beak, Peter
Journal of Organic Chemistry, 1999 , vol. 64, # 5 p. 1705 - 1708
反应条件
triethylamine in dichloromethane T=20°C; 18 h;
参考文献
Wu, Yong-Jin; He, Huan; Sun, Li-Qiang; L'Heureux, Alexandre; Chen, Jie; Dextraze, Pierre; Starrett Jr., John E.; Boissard, Christopher G.; Gribkoff, Valentin K.; Natale, Joanne; Dworetzky, Steven I.
Journal of Medicinal Chemistry, 2004 , vol. 47, # 11 p. 2887 - 2896
反应条件
1: 86 percent / NaH / tetrahydrofuran 2: 1.) n-BuLi, (-)-sparteine / 1.) toluene, -78 deg C, 4 h, 2.) toluene, -78 deg C -> room temperature 3: ammonium cerium(IV) nitrate / acetonitrile; H2O / 0.5 h / 0 °C View Scheme
参考文献
Kim, Bong Jin; Park, Yong Sun; Beak, Peter
Journal of Organic Chemistry, 1999 , vol. 64, # 5 p. 1705 - 1708
反应条件
1: 86 percent / NaH / tetrahydrofuran 2: 1.) n-BuLi, (-)-sparteine / 1.) toluene, -78 deg C, 4 h, 2.) toluene, -78 deg C -> room temperature 3: ammonium cerium(IV) nitrate / acetonitrile; H2O / 0.5 h / 0 °C View Scheme
参考文献
Kim, Bong Jin; Park, Yong Sun; Beak, Peter
Journal of Organic Chemistry, 1999 , vol. 64, # 5 p. 1705 - 1708
反应条件
1: 1.) n-BuLi, (-)-sparteine / 1.) toluene, -78 deg C, 4 h, 2.) toluene, -78 deg C -> room temperature 2: ammonium cerium(IV) nitrate / acetonitrile; H2O / 0.5 h / 0 °C View Scheme
参考文献
Kim, Bong Jin; Park, Yong Sun; Beak, Peter
Journal of Organic Chemistry, 1999 , vol. 64, # 5 p. 1705 - 1708
反应条件
in 3-methyl pentan-3-ol
参考文献
Queyroy, Severine; Vanthuyne, Nicolas; Gastaldi, Stephane; Bertrand, Michele P.; Gil, Gerard
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 9 p. 1759 - 1764
反应条件
1: NaIO4, RuCl3*H2O / CCl4; acetonitrile; H2O / 48 h / Ambient temperature 2: 1.) thionyl chloride, 2.) di-tert-butyl dicarbonate / 1.) 2 h, 2.) CH2Cl2 View Scheme
参考文献
Kim, Bong Jin; Park, Yong Sun; Beak, Peter
Journal of Organic Chemistry, 1999 , vol. 64, # 5 p. 1705 - 1708
反应条件
ruthenium trichloride; sodium periodate in tetrachloromethane; water; acetonitrile 48 h; Ambient temperature;
参考文献
Kim, Bong Jin; Park, Yong Sun; Beak, Peter
Journal of Organic Chemistry, 1999 , vol. 64, # 5 p. 1705 - 1708
反应条件
hydrogenchloride; N-bromosuccinmide in acetone
T=20°C; 2 h;
参考文献
Wu, Yong-Jin; He, Huan; Sun, Li-Qiang; L'Heureux, Alexandre; Chen, Jie; Dextraze, Pierre; Starrett Jr., John E.; Boissard, Christopher G.; Gribkoff, Valentin K.; Natale, Joanne; Dworetzky, Steven I.
Journal of Medicinal Chemistry, 2004 , vol. 47, # 11 p. 2887 - 2896
