3-甲基-2(5H)-呋喃酮合成路线 (共 48 条)
反应条件
potassium carbonate; hydrazine; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=25°C; P=760 Torr; 72 h;
参考文献
Cowell,A.; Stille,J.K.
Journal of the American Chemical Society, 1980 , vol. 102, p. 4193
反应条件
chlorocatecholborane; Grubb's 2nd generation catalyst in dichloromethane T=40°C; 14 h;
参考文献
Moise, Joelle; Arseniyadis, Stellios; Cossy, Janine
Organic Letters, 2007 , vol. 9, # 9 p. 1695 - 1698
反应条件
tri-ruthenium(0)dodecacarbonyl; triethylamine in 1,4-dioxane T=100°C; P=7600 Torr; 8 h;
参考文献
Yoneda, Eiji; Zhang, Shi-Wei; Zhou, Da-Yang; Onitsuka, Kiyotaka; Takahashi, Shigetoshi
Journal of Organic Chemistry, 2003 , vol. 68, # 22 p. 8571 - 8576
反应条件
tributyl-amine; lithium chloride; tetrakis(triphenylphosphine) palladium(0) in acetonitrile P=760 Torr; Heating;
参考文献
Crisp, Geoffrey T.; Meyer, Adam G.
Journal of Organic Chemistry, 1992 , vol. 57, # 25 p. 6972 - 6975
反应条件
carbon monoxide; hydrogen; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in dichloromethane T=100°C; P=31028.9 Torr; 18 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 3 p. 499 - 503
反应条件
sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium(0) in xylene T=130°C; 16 h; Yield given. Yields of byproduct given;
参考文献
Henin, Francoise; Pete, Jean-Pierre
Tetrahedron Letters, 1983 , vol. 24, # 43 p. 4687 - 4690
反应条件
dihydrogen peroxide in dichloromethane T=0 - 20°C; 0.75 h;
参考文献
Patra, Pranab K.; Shanmugasundaram, Kandasamy; Matoba, Manabu; Nishide, Kiyoharu; Kajimoto, Tetsuya; Node, Manabu
Synthesis, 2005 , # 3 art. no. F12504SS, p. 447 - 457
反应条件
hydrogen; (η6-C6H5BPh3)(1-)*Rh(1+)*(1,5-COD); 1,4-di(diphenylphosphino)-butane in dichloromethane T=100°C; P=31028.9 Torr; 18 h; Yields of byproduct given;
参考文献
Lee, Chul Woo; Alper, Howard
Journal of Organic Chemistry, 1995 , vol. 60, # 3 p. 499 - 503
反应条件
C28H32Cl2N2ORu in toluene T=70°C; 18 h; Inert atmosphere;
参考文献
Malik, Heetika; Rutjes, Floris P. J. T.; Zwanenburg, Binne
Synthesis, 2010 , # 19 art. no. T07610SS, p. 3271 - 3273
反应条件
Rhodium trichloride in ethanol 16 h; Heating;
参考文献
Jefford; Sledeski; Rossier; Boukouvalas
Tetrahedron Letters, 1990 , vol. 31, # 40 p. 5741 - 5744