1,3-双(甲氧基甲基)苯合成路线 （共 5 条）
参考文献
Sumika Fine Chemicals Co., Ltd.
Patent: US6310222 B1, 2001 ;
反应条件
in methanol; benzene T=0°C; 3 h; Yields of byproduct given;
参考文献
Nakazaki, Masao; Hirose, Yoshiki; Shimizu, Toru; Suzuki, Takaaki; Ishii, Akira; Makimura, Masaru
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1428 - 1435
反应条件
argentic oxide 0.5 h; Ambient temperatureIrradiation;
参考文献
Ortiz; Walls; Yuste; Barrios; Sanchez-Obregon; Pinelo
Synthetic Communications, 1993 , vol. 23, # 6 p. 749 - 756
参考文献
Wang, Wuyi; Li, Tiechao; Attardo, Giorgio
Journal of Organic Chemistry, 1997 , vol. 62, # 19 p. 6598 - 6602
反应条件
1: (i) NBS, (irradiation), (ii) NaOMe, (iii) aq. HCl
2: (i) NaNH2, liq. NH3, Fe(NO3)3, (ii) /BRN= 2437320/, (iii) aq. HBr
3: (i) NaOAc, AcOH, (ii) (irradiation), (iii) aq. KOH
4: PBr3
5: Na
View Scheme
参考文献
Blaschke,H. et al.
Journal of the American Chemical Society, 1970 , vol. 92, # 12 p. 3675 - 3681
