5-氯苯并-2,1,3-噻二唑合成路线 （共 10 条）
反应条件
thionyl chloride; sulfuric acid 1 h; Heating / reflux;
参考文献
SHOWA DENKO K. K.
Patent: US2009/149676 A1, 2009 ;
Location in patent: Page/Page column 5 ;
参考文献
Doklady Akademii Nauk SSSR, , vol. 106, p. 88,89
Doklady Chemistry, 106-111 <1956> 31, 32
Zhurnal Obshchei Khimii, , vol. 27, p. 1570,1572; engl. Ausg. S. 1643, 1645
反应条件
hydrogenchloride; potassium chlorate Heating;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 34, # 4 p. 1267 - 1272,1265 - 1269
反应条件
methanol; samarium diiodide in tetrahydrofuran T=20°C; 0.25 h;
参考文献
Fan, Xuesen; Zhang, Xinying; Zhang, Yongmin
Journal of Chemical Research, 2005 , # 1 p. 21 - 22
反应条件
1: concentrated HNO3; concentrated H2SO4 2: iron View Scheme
参考文献
Pesin; Chalezkii
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2599,2603; engl. Ausg. S. 2656, 2659
反应条件
sulfuric acid; nitric acid
参考文献
Ghosh,P.B.; Everitt,B.J.
Journal of Medicinal Chemistry, 1974 , vol. 17, # 2 p. 203 - 206
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 34, p. 3028 - 3034,3063 - 3069
反应条件
1: HNO3, H2SO4 2: aq. NaN3 / dimethylsulfoxide 3: P(OEt)3 / Heating View Scheme
参考文献
Ghosh,P.B.; Everitt,B.J.
Journal of Medicinal Chemistry, 1974 , vol. 17, # 2 p. 203 - 206
反应条件
1: HNO3, H2SO4 2: aq. NaN3 / dimethylsulfoxide View Scheme
参考文献
Ghosh,P.B.; Everitt,B.J.
Journal of Medicinal Chemistry, 1974 , vol. 17, # 2 p. 203 - 206
反应条件
t-Bu Brett Phos; C44H62NO5PPdS; sodium t-butanolate in 1,4-dioxane
T=50°C; 20 h; Sealed tubeInert atmosphere;
参考文献
Cheung, Chi Wai; Buchwald, Stephen L.
Organic Letters, 2013 , vol. 15, # 15 p. 3998 - 4001
