5,5-二甲氧基-1,2,3,4-四氯环戊二烯合成路线 (共 20 条)
反应条件
potassium hydroxide T=20°C; 4.5 h; Inert atmosphere;
参考文献
Malihi, Farzad; Clive, Derrick L. J.; Chang, Che-Chien; Minaruzzaman
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 996 - 1013
反应条件
potassium hydroxide T=48 - 60°C;
参考文献
Journal of the American Chemical Society, , vol. 71, p. 946,950
参考文献
Tetrahedron, , vol. 25, p. 1265 - 1280
Journal of Organic Chemistry, , vol. 30, p. 2635 - 2639
参考文献
Mackenzie,K.
Journal of the Chemical Society, 1962 , p. 457 - 463
参考文献
McBee et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 385
参考文献
McBee et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 385
反应条件
in dimethyl sulfoxide T=20°C; 12 h; other alloxide anions; Mechanism;
参考文献
Ismailov, S. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 10.2 p. 2022 - 2023
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 10 p. 2238 - 2240
反应条件
1: 100 percent / K2CO3 / methanol / 0.33 h 2: 88 percent / Na; NH3 / methanol / 1 h View Scheme
参考文献
Clive, Derrick L.J.; Sgarbi, Paulo W.M.; He, Xiao; Sun, Shaoyi; Zhang, Junhu; Ou, Ligong
Canadian Journal of Chemistry, 2003 , vol. 81, # 7 p. 811 - 824
反应条件
potassium hydroxide in dimethyl sulfoxide T=20°C; 18 h;
参考文献
Mackenzie, K.; Proctor, G.; Woodnutt, D. J.
Tetrahedron, 1987 , vol. 43, # 24 p. 5981 - 5994
反应条件
in methanol; dimethyl sulfoxide
参考文献
van Bree,J.; Anteunis,M.J.O.
Bulletin des Societes Chimiques Belges, 1978 , vol. 87, p. 135 - 142