2-重氮基-2-苯基乙酸乙酯合成路线 （共 16 条）
反应条件
tetrabutylammomium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=45°C; 12 h;
参考文献
Peng, Cheng; Cheng, Jiajia; Wang, Jianbo
Journal of the American Chemical Society, 2007 , vol. 129, # 28 p. 8708 - 8709
反应条件
4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=20°C;
参考文献
Hu, Mingyou; He, Zhengbiao; Gao, Bing; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17302 - 17305
反应条件
1: With benzoic acid; hydrazine in tetrahydrofuran T=20°C; 16 h; 2: With N-iodo-N-potassio-p-toluenesulphonamide; potassium hydroxide in tetrahydrofuran; water T=20°C;
参考文献
Nicolle, Simon M.; Moody, Christopher J.
Chemistry - A European Journal, 2014 , vol. 20, # 15 p. 4420 - 4425
反应条件
1: With sodium hydride in diethyl ether 2: With 4-toluenesulfonyl azide in diethyl ether 0.75 h;
参考文献
Bachmann, Stephan; Fielenbach, Doris; Jorgensen, Karl Anker
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 20 p. 3044 - 3049
反应条件
sodium; ethylene glycol T=70 - 75°C;
参考文献
Journal of Organic Chemistry, , vol. 51, # 14 p. 2664 - 2668
反应条件
4-toluenesulfonyl azide; triethylamine in dichloromethane
参考文献
Chemische Berichte, , vol. 101, # 8 p. 2622 - 2632
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 9 p. 2404 - 2408
反应条件
bis-triphenylphosphine-palladium(II) chloride; trifuran-2-yl-phosphane 1) THF, rt, 20 min; 2) THF, reflux, 4 h; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 53, # 7 p. 2371 - 2386
反应条件
bis-triphenylphosphine-palladium(II) chloride; trifuran-2-yl-phosphane 1) THF, rt, 20 min; 2) THF, reflux, 4 h; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 53, # 7 p. 2371 - 2386
反应条件
water; copper(II) sulfate in chloroform T=40°C; 0.5 h; Title compound not separated from byproducts.;
参考文献
Zhu, Shou-Fei; Chen, Chao; Cai, Yan; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2008 , vol. 47, # 5 p. 932 - 934
