1,1,1,2,3,3,3-七氟-2-甲氧基丙烷合成路线 (共 4 条)
反应条件
cesium fluoride in bis [2-(2-methoxyethoxy)ethyl] ether T=100°C; 36 h;
参考文献
Solvay Solexis S.p.A.
Patent: US2004/192974 A1, 2004 ;
Location in patent: Page 5 ;
反应条件
cesium fluoride in N,N-dimethyl-formamide T=20°C; 3 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Rogovik, V. M.; Delyagina, N. I.; Mysov, E. I.; Cherstkov, V. F.; Sterlin, S. R.; German, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 9.1. p. 1870 - 1876
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 9 p. 2057 - 2063
反应条件
in acetonitrile-D3 T=20°C; 0.5 h; Product distribution; Further Variations:Temperaturestime;
参考文献
Suzuta, Tetsuya; Abe, Takashi; Sekiya, Akira
Journal of Fluorine Chemistry, 2003 , vol. 119, # 1 p. 3 - 8
反应条件
T=85 - 90°C; 12 h; Product distribution;
参考文献
Kadyrov, A. A.; Rokhlin, E. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, p. 1224 - 1230
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 6 p. 1353 - 1359