3-(吡咯烷-1-基)丙酸甲酯合成路线 (共 10 条)
反应条件
zirconium tetrachloride in dichloromethane T=20°C; Michael addition; 0.75 h;
参考文献
Groselj, Uros; Kralj, David; Wagger, Jernej; Dahmann, Georg; Stanovnik, Branko; Svete, Jurij
Arkivoc, 2012 , vol. 2012, # 3 p. 49 - 65
反应条件
9,10-anthracenedione in acetonitrile T=5°C; 2 h; Irradiation; Yields of byproduct given;
参考文献
Das, Suresh; Kumar, J. S. Dileep; Shivaramayya, K.; George, M. V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 14 p. 1797 - 1800
反应条件
in tetrahydrofuran; methanol Heating;
参考文献
Anjaiah, Siddam; Chandrasekhar, Srivari; Gree, Rene
Tetrahedron Letters, 2004 , vol. 45, # 3 p. 569 - 571
反应条件
in benzene 5 h; Heating; Yield given. Yields of byproduct given;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 19, # 11 p. 1197 - 1201
Khimiya Geterotsiklicheskikh Soedinenii, , # 11 p. 1510 - 1514
反应条件
1: 85 percent / lithium aluminium hydride / diethyl ether / 1 h 2: thionyl chloride / CH2Cl2 / 2.5 h / cooling View Scheme
参考文献
Le Sann, Christine; Baron, Anne; Mann, John; Van Den Berg, Hendrik; Gunaratnam, Mekala; Neidle, Stephen
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 7 p. 1305 - 1312
反应条件
hydrogen fluoride T=7 - 8°C; 9.96667 h; electrochemical fluorination;
参考文献
Abe, Takashi; Hayashi, Eiji; Fukaya, Haruhiko; Hayakawa, Yoshio; Baba, Hajime; et al.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 101 - 111
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C; 2 h;
参考文献
Le Sann, Christine; Huddleston, Jonathan; Mann, John
Tetrahedron, 2007 , vol. 63, # 52 p. 12903 - 12911
反应条件
1: With sodium hydroxide in water T=20°C; 2 h; 2: With hydrogenchloride T=20°C; 0.25 h;
参考文献
Groselj, Uros; Kralj, David; Wagger, Jernej; Dahmann, Georg; Stanovnik, Branko; Svete, Jurij
Arkivoc, 2012 , vol. 2012, # 3 p. 49 - 65
反应条件
hydrogen fluoride T=7 - 8°C; 9.96667 h; electrochemical fluorination;
参考文献
Abe, Takashi; Hayashi, Eiji; Fukaya, Haruhiko; Hayakawa, Yoshio; Baba, Hajime; et al.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 101 - 111
反应条件
ethanol; hydrazine hydrate
T=80°C;
参考文献
Dow Chem. Co.
Patent: US2834781 , 1956 ;