1: With triethylamine in dichloromethane T=20°C; 50 h; 2: With ammonium fluoride in methanol T=10°C; 3 h; Title compound not separated from byproducts;
参考文献
Tishkov, Alexander A.; Lyapkalo, Il'ya M.; Ioffe, Sema L.; Strelenko, Yuri A.; Tartakovsky, Vladimir A.
Tetrahedron, 2001 , vol. 57, # 11 p. 2221 - 2230
sodium dithionite; potassium carbonate; N,N'-dioctyl-4,4'-bipyridinium in dichloromethane; water
T=35°C; 3 h;
参考文献
Park, Kwanghee Koh; Lee, Chul Woo; Choi, Sook Young
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 5 p. 601 - 604
v.Schickh
Angewandte Chemie, 1950 , vol. 62, p. 547,554
Full Text Show Details
Shechter et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 3664,3666,3667
in water
Michael Addition; pH=6.9; 4 h; RefluxGreen chemistry;
参考文献
Giorgi, Giorgio; Lopez-Alvarado, Pilar; Miranda, Sonia; Rodriguez, Jean; Menendez, J. Carlos
European Journal of Organic Chemistry, 2013 , # 7 p. 1327 - 1336