3,4,5-三苯基异恶唑合成路线 （共 47 条）
反应条件
2,2'-azo-bisisobutyronitrile in dimethyl sulfoxide
T=80°C; 2 h;
参考文献
Fukunaga, Kimitoshi; Okamoto, Akihiko; Furumoto, Keiji; Kimura, Makoto
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 9 p. 3045 - 3046
反应条件
potassium hydroxide; iodine in ethanol
T=25 - 60°C;
参考文献
Badea, Florin; Iordache, Florin; Costea, Ion; Iordache, Stefan; Meghea, Aurelia; Simion, Alina; Simion, Cristian
Revue Roumaine de Chimie, 2000 , vol. 45, # 4 p. 361 - 368
反应条件
sodium hydroxide in water
3 h; Heating;
参考文献
Crombie, Leslie; Roughley, Brian S.
Tetrahedron, 1986 , vol. 42, # 12 p. 3147 - 3156
反应条件
sodium in ethanol
boiling;
参考文献
Gmelin Handbook: Fe: Org.Verb.A4, 5.1.4.1.4.2, page 69 - 80
反应条件
1: nitrogen dioxide / benzene
2: 30percent sodium hydroxide / H2O / 3 h / Heating
View Scheme
参考文献
Crombie, Leslie; Roughley, Brian S.
Tetrahedron, 1986 , vol. 42, # 12 p. 3147 - 3156
反应条件
1: 69 percent / N-bromosuccinimide / benzene / 20 - 25 °C
2: 88 percent / silver nitrate / ethanol; H2O / heated on a steam bath
View Scheme
参考文献
Hansen, John F.; Kim, Yong In; McCrotty, Stephen E.; Strong, Scott A.; Zimmer, Douglas E.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 475 - 479
反应条件
hydrogenchloride; hydroxylamine hydrochloride; acetic acid
T=200°C; im Rohr;
参考文献
Meisenheimer; Weibezahn
Chemische Berichte, 1921 , vol. 54, p. 3200
反应条件
1: benzene
2: aqueous NaOH
View Scheme
参考文献
Brown; Shriner
Journal of Organic Chemistry, 1937 , vol. 2, p. 376,380
反应条件
lithium methanolate; bromine
1.) DMF, 15 min, 2.) DMF, ice-cooling, then room temp., 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Crombie, Leslie; Roughley, Brian S.
Tetrahedron, 1986 , vol. 42, # 12 p. 3147 - 3156
反应条件
bei der Destillation im Vakuum;
参考文献
Kohler, Barrett
Journal of the American Chemical Society, 1924 , vol. 46, p. 2105
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Meisenheimer; Weibezahn
Chemische Berichte, 1921 , vol. 54, p. 3200
Full Text Show Details
Heim
Chemische Berichte, 1911 , vol. 44, p. 2017
