2,5-二甲基吡咯-3-乙酯合成路线 （共 32 条）
反应条件
sodium azide in tert-butyl alcohol T=65°C; 20 h;
参考文献
Huang, Xian; Shen, Ruwei; Zhang, Tiexin
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1534 - 1537
反应条件
trimethylsilyl trifluoromethanesulfonate in nitromethane T=-40°C; 9 h;
参考文献
Yu, Ming; Pagenkopf, Brian L.
Organic Letters, 2003 , vol. 5, # 26 p. 5099 - 5101
反应条件
diisobutylaluminium hydride in tetrahydrofuran T=-20°C; 1 h;
参考文献
Alberola, Angel; Ortega, Alfonso Gonzalez; Sadaba, M. Luisa; Sanudo, Carmen
Tetrahedron, 1999 , vol. 55, # 21 p. 6555 - 6566
反应条件
in tert-butyl alcohol T=80°C; 3 h;
参考文献
Huang, Xian; Shen, Ruwei; Zhang, Tiexin
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1534 - 1537
反应条件
sodium azide in water; tert-butyl alcohol T=20°C; 48 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 4 p. 1534 - 1537
反应条件
copper acetylacetonate in dichloromethane T=55 - 60°C; 72 h;
参考文献
Augusti, Rodinei; Eberlin, Marcos N.; Kascheres, Concetta
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 4 p. 1355 - 1358
反应条件
copper acetylacetonate in dichloromethane T=55 - 60°C; 72 h;
参考文献
Augusti, Rodinei; Eberlin, Marcos N.; Kascheres, Concetta
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 4 p. 1355 - 1358
反应条件
N,N'-dimethylhydrazine bishydrochloride 120 h;
参考文献
Inel, Sermin; Jones, R. Alan; Ogretir, Cemil
Tetrahedron, 1984 , vol. 40, # 20 p. 3979 - 3986
反应条件
1: methanol / 20 h / 20 °C 2: 74 percent / DIBAL-H / tetrahydrofuran / 1 h / -20 °C View Scheme
参考文献
Tetrahedron, , vol. 55, # 21 p. 6555 - 6566
参考文献
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, , vol. 121, p. 146
