5-甲氧基-3-甲基-1H-吲哚合成路线 (共 21 条)
反应条件
ammonia; sodium in tetrahydrofuran T=-33°C; 1.5 h;
参考文献
Trost, Barry M.; Quancard, Jean
Journal of the American Chemical Society, 2006 , vol. 128, # 19 p. 6314 - 6315
反应条件
hydrogen; acetic acid; 10 palladium on active carbon in ethanol P=2280 Torr; 2 h; Ambient temperature;
参考文献
Makosza, Mieczyslaw; Danikiewicz, Witold; Wojciechowski, Krzysztof
Liebigs Annalen der Chemie, 1988 , p. 203 - 208
反应条件
carbon monoxide; [Rh(CO)2(Me2NCH2CH2NMe2)][RhCl2(CO)2] in tetrahydrofuran T=100°C; P=5171.62 Torr; 20 h; Autoclave;
参考文献
Okuro, Kazumi; Gurnham, Joanna; Alper, Howard
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4715 - 4720
反应条件
palladium in ethanol
反应条件
diisobutylaluminium hydride in benzene T=0°C; 1.5 h;
参考文献
Marino; Hurt
Synthetic Communications, 1994 , vol. 24, # 6 p. 839 - 848
反应条件
tin(ll) chloride; ruthenium trichloride; triphenylphosphine in 1,4-dioxane T=180°C; 20 h; Yield given. Yields of byproduct given;
参考文献
Chemical Communications, , # 9 p. 995 - 996
反应条件
quinoline; copper 2.5 h; Heating;
参考文献
Zhao, Shuo; Liao, Xuebin; Wang, Tao; Flippen-Anderson, Judith; Cook, James M.
Journal of Organic Chemistry, 2003 , vol. 68, # 16 p. 6279 - 6295
反应条件
1.1: triethylamine / 1.5 h / 80 °C 1.2: 68 percent / ZnCl2 / ethanol / 4 h / 110 °C 2.1: 83 percent / Na; NH3 / tetrahydrofuran / 1.5 h / -33 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 19 p. 6314 - 6315
反应条件
1: 85 percent / t-BuOK / dimethylformamide / 2.5 h / -23 °C 2: 98 percent / K2CO3, 18-crown-6 / acetonitrile / 12 h / Heating 3: 99 percent / H2 / PtO2 / aq. ethanol; ethyl acetate 4: 70 percent / DIBALH / benzene / 1.5 h / 0 °C View Scheme
参考文献
Synthetic Communications, , vol. 24, # 6 p. 839 - 848
反应条件
1: 100 percent / KOH / ethanol / 1 h / Heating 2: 93.6 percent / Cu; quinoline / 2.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 16 p. 6279 - 6295