1,1,1,3,3-五氯丁烷合成路线 （共 11 条）
反应条件
zinc in N,N-dimethyl-formamide T=25 - 30°C; Title compound not separated from byproducts;
参考文献
Doklady Chemistry, , vol. 260, p. 442 - 445
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 260, # 6 p. 1370 - 1374
反应条件
ECOENG(TM)212; copper(l) iodide
T=130°C; Product distribution / selectivity;
参考文献
SOLVAY (Societe Anonyme)
Patent: WO2008/43720 A2, 2008 ;
Location in patent: Page/Page column 16 ;
反应条件
pentacarbonyliron(0); propene in N,N-dimethyl-formamide; isopropyl alcohol
T=130°C; 1.5 h; Further byproducts given. Yields of byproduct given;
参考文献
Grigor'ev, N. A.; Kuz'mina, N. A.; Chukovskaya, E. Ts.; Tumanskaya, A. L.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 6 p. 952 - 955
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 6 p. 1333 - 1336
反应条件
pentacarbonyliron(0); [14C]-1,1-Dichloroethylene in N,N-dimethyl-formamide
T=130°C; 1.5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Grigor'ev, N. A.; Kuz'mina, N. A.; Chukovskaya, E. Ts.; Tumanskaya, A. L.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 6 p. 952 - 955
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 6 p. 1333 - 1336
反应条件
pentacarbonyliron(0) in N,N-dimethyl-formamide
T=130°C; 1.5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Grigor'ev, N. A.; Kuz'mina, N. A.; Chukovskaya, E. Ts.; Tumanskaya, A. L.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 6 p. 952 - 955
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 6 p. 1333 - 1336
反应条件
pentacarbonyliron(0); N,N-dimethyl-formamide
T=150°C; 2.5 h;
参考文献
Vasil'eva, T. T.; Velichko, F. K.; Trapeznikova, G. A.; Abdulkina, Z. A.; Amriev, R. A.; Nelyubin, B. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 5 p. 835 - 841
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 5 p. 1075 - 1081
参考文献
Bekhazi, Michel; Warkentin, John
Canadian Journal of Chemistry, 1983 , vol. 61, p. 619 - 624
反应条件
aluminium trichloride
参考文献
Kulikova,A.E. et al.
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, p. 1899 - 1904,1834 - 1838
参考文献
Bekhazi, Michel; Warkentin, John
Canadian Journal of Chemistry, 1983 , vol. 61, p. 619 - 624
反应条件
pentacarbonyliron(0); N,N-dimethyl-formamide
T=130°C; 4 h; other time; Product distribution;
参考文献
Vasil'eva, T. T.; Velichko, F. K.; Trapeznikova, G. A.; Abdulkina, Z. A.; Amriev, R. A.; Nelyubin, B. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 5 p. 835 - 841
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 5 p. 1075 - 1081
