2,3-二甲基萘-1,4-二酮合成路线 (共 85 条)
反应条件
2: HBr, AcOH
3: aq. FeCl3, H+ / ethanol
4: 180 °C
View Scheme
参考文献
Manecke,G. et al.
Chemische Berichte, 1967 , vol. 100, p. 836 - 844
反应条件
copper(II) sulfate
T=50°C; 1 h;
参考文献
Bansal; Thapliyal; Khanna
Synthetic Communications, 1995 , vol. 25, # 11 p. 1669 - 1675
反应条件
(NH4)2S2O8; silver nitrate in acetonitrile
参考文献
Sharma,S.C.; Torssell,K.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1978 , vol. 32, p. 347 - 353
反应条件
1: 44 percent
2: 2.) air / 1.) xylene, 160 deg C, 5 min
View Scheme
参考文献
Liebeskind, Lanny S.; Iyer, Suresh; Jewell, Charles F.
Journal of Organic Chemistry, 1986 , vol. 51, # 15 p. 3065 - 3067
反应条件
in benzene
Irradiation;
参考文献
Osuka, Atsuhiro; Suzuki, Hitomi; Maruyama, Kazuhiro
Chemistry Letters, 1981 , p. 201 - 204
反应条件
sodium peroxodisulphate; sulfuric acid; silver nitrate in water
4 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Minisci, Francesco; Coppa, Fausta; Fontana, Francesca; Zhao, Lihua
Gazzetta Chimica Italiana, 1993 , vol. 123, # 11 p. 613 - 616
反应条件
triethylamine in benzene
Irradiation; Product distribution;
参考文献
Maruyama, Kazuhiro; Otsuki, Tetsuo; Osuka, Atsuhiro; Suzuki, Hitomi
Chemistry Letters, 1982 , p. 1 - 4
反应条件
isopropyl alcohol in benzene
Irradiationwithout solvent; Product distribution;
参考文献
Osuka, Atsuhiro; Suzuki, Hitomi; Maruyama, Kazuhiro
Chemistry Letters, 1981 , p. 201 - 204
反应条件
sodium peroxodisulphate; sulfuric acid; silver nitrate in water; acetonitrile
4 h; Heating; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Minisci, Francesco; Coppa, Fausta; Fontana, Francesca; Zhao, Lihua
Gazzetta Chimica Italiana, 1993 , vol. 123, # 11 p. 613 - 616
反应条件
in acetic acid
0.0833333 h; Ambient temperature;
参考文献
Greenland, Harry; Pinhey, John T.; Sternhell, Sever
Australian Journal of Chemistry, 1986 , vol. 39, p. 2067 - 2074