2,3-二甲基萘-1,4-二酮合成路线 (共 85 条)
反应条件
hydrogenchloride; amalgamated zinc higher-boiling 2.3-dimethyl-tetralin;
参考文献
Madinaveitia
Anales de la Real Sociedad Espanola de Fisica y Quimica, 1934 , vol. 32, p. 1100,1105
Chem. Zentralbl., 1935 , vol. 106, # I p. 3134
反应条件
in methanol; benzene 4 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 282 - 288
反应条件
in methanol; benzene 8 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 282 - 288
反应条件
chromium(VI) oxide; periodic acid in acetonitrile
T=5°C; 1 h;
参考文献
Yamazaki, Shigekazu
Tetrahedron Letters, 2001 , vol. 42, # 19 p. 3355 - 3357
反应条件
chromium(VI) oxide in acetic acid
T=50°C; Oxidation; 0.75 h;
参考文献
Schmid, Ralf; Goebel, Friederike; Warnecke, Andre; Labahn, Andreas
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 6 p. 1199 - 1202
反应条件
tert.-butylhydroperoxide; poly(bis-1,2-phenylene) diselenide in tert-butyl alcohol
T=80°C; 72 h;
参考文献
Wojtowicz, Halina; Mlochowski, Jacek; Syper, Ludwik; Yadav, Hardeo
Synthetic Communications, 2006 , vol. 36, # 14 p. 1991 - 2000
反应条件
(NH4)2S2O8; silver nitrate in water; acetonitrile
0.5 h; Heating15 mol eq. acetic acid;
参考文献
Ashnagar, Alamdar; Bruce, J. Malcolm; Lloyd-Williams, Paul
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 559 - 562
反应条件
copper(II) sulfate
T=50°C; 2 h;
参考文献
Bansal; Thapliyal; Khanna
Synthetic Communications, 1995 , vol. 25, # 11 p. 1669 - 1675
反应条件
trifluoroacetic acid; ethanethiol
26 h; Ambient temperature;
参考文献
Silverman
Journal of the American Chemical Society, 1981 , vol. 103, # 19 p. 5939 - 5941
反应条件
(NH4)2S2O8; silver nitrate in water; acetonitrile
T=65°C; Kochi-Anderson procedure;
参考文献
Commandeur, Claude; Chalumeau, Celine; Dessolin, Jean; Laguerre, Michel
European Journal of Organic Chemistry, 2007 , # 18 p. 3045 - 3052