5-溴-3-(邻苯二甲酰亚氨基甲基)吡啶合成路线 （共 3 条）
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=20°C; Mitsunobu reaction;
参考文献
Bhatti, Balwinder S.; Strachan, Jon-Paul; Breining, Scott R.; Miller, Craig H.; Tahiri, Persida; Crooks, Peter A.; Deo, Niranjan; Day, Cynthia S.; Caldwell, William S.
Journal of Organic Chemistry, 2008 , vol. 73, # 9 p. 3497 - 3507
反应条件
1: sodium tetrahydroborate / methanol / 2 h / 0 - 20 °C 2: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / tetrahydrofuran / 6 h / 20 °C View Scheme
参考文献
Samumed, LLC; Hood, John; Kumar KC, Sunil; Wallace, David Mark
Patent: US2013/296302 A1, 2013 ;
反应条件
hydrazine hydrate in ethanol T=70°C; 3 h;
参考文献
US2013/267495 A1, ;
Paragraph 0457 ;
