2-氯-4-甲氧基苯乙酮合成路线 (共 91 条)
反应条件
hydrogenchloride; ammonium nitrate; iodine; oxygen in water; acetonitrile T=60°C; 72 h; Green chemistryLarge scale; Solvent; chemoselective reaction;
参考文献
Prebil, Rok; Stavber, Stojan
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 6 p. 1266 - 1274
反应条件
aluminium trichloride in dichloromethane 2 h; Ambient temperature;
参考文献
Giordano, Claudio; Castaldi, Graziano; Casagrande, Francesco; Belli, Aldo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 11 p. 2575 - 2582
反应条件
[2,2']bipyridinyl; copper(l) chloride in 1,2-dichloro-ethane 3 h; Heating;
参考文献
Ram, Ram N.; Manoj
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5633 - 5635
反应条件
ruthenium (2+) in benzene T=120°C; 7 h; sealed;
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Yoshikawa, Manabu; Shimizu, Toshio
Journal of Organometallic Chemistry, 1998 , vol. 552, # 1-2 p. 39 - 43
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; trifluoromethane sulfonylchloride in benzene T=120°C; 7 h;
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Shimizu, Toshio
Phosphorus, Sulfur and Silicon and Related Elements, 1997 , vol. 129, p. 155 - 168
反应条件
ethylmagnesium bromide in tetrahydrofuran T=-70 - -40°C; 2 h;
参考文献
Satoh Tsuyoshi; Mizu, Yasuhiro; Kawashima, Taku; Yamakawa, Koji
Tetrahedron, 1995 , vol. 51, # 3 p. 703 - 710
反应条件
aluminum oxide; sodium chlorite; Mn(III) acetylacetonate in dichloromethane T=20°C; 3.16667 h;
参考文献
Synthetic Communications, , vol. 28, # 1 p. 131 - 138
反应条件
hydrogenchloride; potassium permanganate in acetonitrile T=60°C;
参考文献
Journal of the Chinese Chemical Society (Taipei, Taiwan), , vol. 44, # 3 p. 309 - 312
反应条件
P2O5/silica gel in 1,2-dichloro-ethane Friedel Crafts acylation; 3 h; Reflux;
参考文献
Tetrahedron Letters, , vol. 49, # 47 p. 6715 - 6719
反应条件
hydrogenchloride; ammonium nitrate; iodine; oxygen in water; acetonitrile T=60°C; 24 h; Green chemistry; regioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 356, # 6 p. 1266 - 1274