in diethyl ether; benzene byproducts: LiCl; addn. of SnCl4 in benzene under of air and moisture to a soln. of LiN(C2H5)2 in ether; reflux for 4 h; filtration;; solvent distd. off; distn. of the residue in high vac.;;
参考文献
Jones, K.; Lappert, M. F.
Journal of the Chemical Society, 1965 , p. 1944 - 1951
Sommer, R.; Schneider, B.; Neumann, W. P.
Liebigs Annalen der Chemie, 1966 , vol. 692, p. 12 - 21
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2.4.5, page 34 - 36
Sommer, R.; Schneider, B.; Neumann, W. P.
Liebigs Annalen der Chemie, 1966 , vol. 692, p. 12 - 21
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2.4.5, page 34 - 36
