7,4'-二羟基-3'-甲氧基异黄酮合成路线 （共 10 条）
反应条件
methanesulfonyl chloride in N,N-dimethyl-formamide T=60 - 70°C; 1.5 h;
参考文献
Waehaelae, Kristiina; Hase, Tapio A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3005 - 3008
反应条件
NADPH disodium salt; β-D-galactose in dimethyl sulfoxide T=30°C; 72 h; Microbiological reaction;
参考文献
Chemler, Joseph A.; Lim, Chin Giaw; Daiss, John L.; Koffas, Mattheos A.G.
Chemistry and Biology, 2010 , vol. 17, # 4 p. 392 - 401
反应条件
1: T=50°C; 0.166667 h; 2: With methanesulfonyl chloride in N,N-dimethyl-formamide T=80°C; 0.5 h;
参考文献
Goto, Hideyuki; Terao, Yoshiyasu; Akai, Shuji
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 4 p. 346 - 360
反应条件
1: H2 / 10percent Pd-C / aq. ethanol 2: 99 percent / BF3*Et2O / 1 h / 60 - 70 °C 3: 94 percent / methanesulphonyl chloride / dimethylformamide / 1.5 h / 60 - 70 °C View Scheme
参考文献
Waehaelae, Kristiina; Hase, Tapio A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3005 - 3008
反应条件
1: 10percent KOH / methanol; H2O 2: H2 / 10percent Pd-C / aq. ethanol 3: 99 percent / BF3*Et2O / 1 h / 60 - 70 °C 4: 94 percent / methanesulphonyl chloride / dimethylformamide / 1.5 h / 60 - 70 °C View Scheme
参考文献
Waehaelae, Kristiina; Hase, Tapio A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3005 - 3008
反应条件
thallium(III) nitrate in methanol 4 h; Ambient temperature;
参考文献
Nabaei-Bidhendi; Bannerjee
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 43 - 45
反应条件
1: 99 percent / BF3*Et2O / 1 h / 60 - 70 °C 2: 94 percent / methanesulphonyl chloride / dimethylformamide / 1.5 h / 60 - 70 °C View Scheme
参考文献
Waehaelae, Kristiina; Hase, Tapio A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3005 - 3008
反应条件
1: 2.0 g / K2CO3 / acetone / 2 h / Heating 2: 0.3 g / thallium(III) trinitrate / methanol / 4 h / Ambient temperature View Scheme
参考文献
Nabaei-Bidhendi; Bannerjee
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 43 - 45
反应条件
1: 1) aq. KOH, 2) dil. HCl / 1) EtOH, 48 h, room temp. 2: 2.0 g / K2CO3 / acetone / 2 h / Heating 3: 0.3 g / thallium(III) trinitrate / methanol / 4 h / Ambient temperature View Scheme
参考文献
Nabaei-Bidhendi; Bannerjee
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 43 - 45
反应条件
1: 3.5 g / K2CO3 / acetone / 1 h / Heating 2: 1) aq. KOH, 2) dil. HCl / 1) EtOH, 48 h, room temp. 3: 2.0 g / K2CO3 / acetone / 2 h / Heating 4: 0.3 g / thallium(III) trinitrate / methanol / 4 h / Ambient temperature View Scheme
参考文献
Nabaei-Bidhendi; Bannerjee
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 43 - 45
