4-氯-9H-噻吨-9-酮合成路线 (共 5 条)
反应条件
AlCl3, aluminium chloride in 1,2-dichloro-ethane T=40 - 45°C; Friedel Crafts Acylation; 1 h;
参考文献
Berg, Carsten
Patent: US2003/229233 A1, 2003 ;
Location in patent: Page 4 ;
反应条件
chlorine in N-methyl-acetamide; chlorobenzene
参考文献
The Sherwin-Williams Company
Patent: US4101558 A1, 1978 ;
反应条件
trifluorormethanesulfonic acid; ytterbium(III) triflate Friedel Crafts reaction; 0.0666667 h; Neat (no solvent)Microwave irradiation;
参考文献
Li, Jie; Jin, Can; Su, Weike
Heterocycles, 2011 , vol. 83, # 4 p. 855 - 866
反应条件
1: methanol. sodium methylate; copper-powder 2: concentrated sulfuric acid View Scheme
参考文献
Mahishi et al.
Journal of the Karnatak University, 1957 , vol. 2, p. 50,57
反应条件
1: methanol. sodium methylate; copper-powder 2: concentrated sulfuric acid View Scheme
参考文献
Mahishi et al.
Journal of the Karnatak University, 1957 , vol. 2, p. 50,57