6-甲醛-吡啶-2-甲酸乙酯合成路线 (共 3 条)
反应条件
1: With selenium(IV) oxide; acetic acid 48 h; Heating / reflux; 2: With sodium hydrogencarbonate in water pH=6;
参考文献
WO2008/91681 A2, ;
Page/Page column 229 ;
反应条件
sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine in dichloromethane T=4 - 20°C; Parikh-Doering oxidation;
参考文献
Organic Process Research and Development, , vol. 14, # 4 p. 820 - 831
反应条件
1: sodium tetrahydroborate / ethanol / 20 °C 2: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 4 - 20 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 14, # 4 p. 820 - 831