2-邻苯二甲酰亚氨基丙酸合成路线 (共 10 条)
参考文献
Chemische Berichte, , vol. 75, p. 1558,1567
Journal of Organic Chemistry, , vol. 23, p. 1335,1337
反应条件
1,5-diazabicyclo[5.4.0]undeca-5-ene in ethanol T=78°C; 1 h; Heating;
参考文献
Andres, Jose Angel; Palomo, Claudio
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 11-12 p. 369 - 371
反应条件
acetic acid 4 h; Heating;
参考文献
Zav'yalov; Dorofeeva; Rumyantseva; Kulikova; Ezhova; Kravchenko; Zavozin
Pharmaceutical Chemistry Journal, 2002 , vol. 36, # 8 p. 440 - 442
反应条件
hydrogenchloride; bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine 1.) benzene, 23 deg C, 25h.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 31, # 33 p. 4783 - 4786
反应条件
bis(1,5-cyclooctadiene)nickel (0); Ni(COD)2 Me2Phen 1.) THF, 23 deg C, 5 h; 2.) THF; Yield given. Multistep reaction;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 103, # 9-10 p. 549 - 558
反应条件
bis(1,5-cyclooctadiene)nickel (0); Me2Phen 1.) THF, 23 deg C, 5 h; 2.) THF; Yield given. Multistep reaction;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 103, # 9-10 p. 549 - 558
反应条件
bis(1,5-cyclooctadiene)nickel (0); Me2Phen 1.) THF, 23 deg C, 5 h; 2.) THF; different alkyl halides and alkynes; Product distributionMechanism;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 103, # 9-10 p. 549 - 558
反应条件
acrylic acid methyl ester in acetonitrile 8 h; Irradiation; Further byproducts given;
参考文献
Yoon, Ung Chan; Kim, Dong Uk; Lee, Chan Woo; Choi, Young Sun; Lee, Yean-Jang; Ammon, Herman L.; Mariano, Patrick S.
Journal of the American Chemical Society, 1995 , vol. 117, # 10 p. 2698 - 2710
反应条件
in acetonitrile 8 h; Irradiation; Further byproducts given;
参考文献
Yoon, Ung Chan; Kim, Dong Uk; Lee, Chan Woo; Choi, Young Sun; Lee, Yean-Jang; Ammon, Herman L.; Mariano, Patrick S.
Journal of the American Chemical Society, 1995 , vol. 117, # 10 p. 2698 - 2710
反应条件
1: 4-(N,N-dimethylamino)pyridinium chlorosulphite chloride / CH2Cl2 / 0.33 h / -20 °C 2: 4-(N,N-dimethylamino)pyridine / CH2Cl2 / 0.42 h / -10 °C View Scheme
参考文献
Arrieta, A.; Garcia, T.; Palomo, C.
Synthetic Communications, 1982 , vol. 12, # 14 p. 1139 - 1146