4-甲氧基苯甲醛二甲缩醛合成路线 （共 70 条）
反应条件
sodium methylate; lithium perchlorate; TDBPA in dichloromethane
indirect electrochemical oxidation;
参考文献
Brinkhaus, Karl-Heinz Grosse; Steckhan, Eberhard; Degner, Dieter
Tetrahedron, 1986 , vol. 42, # 2 p. 553 - 560
反应条件
potassium fluoride
Electrochemical reactionContinuous flow conditions;
参考文献
Bouzek, Karel; Jiricny, Vladimir; Kodym, Roman; Kristal, Jiri; Bystron, Tomas
Electrochimica Acta, 2010 , vol. 55, # 27 p. 8172 - 8181
反应条件
camphor-10-sulfonic acid in dichloromethane
T=20°C; 2 h;
参考文献
Ko, Haye Min; Lee, Dong Gil; Kim, Min Ah; Kim, Hak Joong; Park, Jaejoon; Lah, Myoung Soo; Lee, Eun
Tetrahedron, 2007 , vol. 63, # 26 p. 5797 - 5805
反应条件
magnesium sulfate; toluene-4-sulfonic acid in toluene
T=90°C; 2.5 h; Inert atmosphere;
参考文献
Hernandez, Dacil; Lindsay, Karl B.; Nielsen, Lone; Mittag, Tina; Bjerglund, Klaus; Friis, Stig; Mose, Rasmus; Skrydstrup, Troels
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3283 - 3293
反应条件
sodium methylate; benzenesulfonic acid potassium salt; TDBPA
参考文献
Brinkhaus, Karl-Heinz Grosse; Steckhan, Eberhard; Degner, Dieter
Tetrahedron, 1986 , vol. 42, # 2 p. 553 - 560
反应条件
indium trifluoromethanesulfonate
T=20°C; 0.5 h; Neat (no solvent);
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
反应条件
1.1: t-BuLi / tetrahydrofuran; pentane / 0.5 h / -78 °C
1.2: I2 / tetrahydrofuran; pentane / 2 h / -78 °C
2.1: 32.6 g / aq. HCl / methanol / 0.5 h
3.1: 99 percent / KMnO4; (n-Bu)4NBr / CH2Cl2 / 24 h / 20 °C
View Scheme
参考文献
Liang, Pi-Hui; Hsin, Ling-Wei; Pong, Sung-Ling; Hsu, Chia-Huei; Cheng, Chen-Yu
Journal of the Chinese Chemical Society, 2003 , vol. 50, # 3 A p. 449 - 456
反应条件
trimethylsilyl cyanide; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in acetonitrile
Ambient temperature;
参考文献
Soga, Tsunehiko; Takenoshita, Haruhiro; Yamada, Masaaki; Mukaiyama, Teruaki
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 11 p. 3122 - 3131
反应条件
ethenetetracarbonitrile in acetonitrile
1 h; Heating;
参考文献
Miura, Tsuyoshi; Masaki, Yukio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 17 p. 2155 - 2158
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=-78 - 0°C; 3 h;
参考文献
Brown, Eric; Dujardin, Gilles; Maudet, Mickael
Tetrahedron, 1997 , vol. 53, # 28 p. 9679 - 9694
