4-甲氧基苯甲醛二甲缩醛合成路线 （共 70 条）
反应条件
toluene-4-sulfonic acid in acetonitrile T=20°C;
参考文献
Xia, Jie; Srikrishnan; Alderfer, James L.; Jain; Piskorz, Conrad F.; Matta, Khushi L.
Carbohydrate Research, 2000 , vol. 329, # 3 p. 561 - 577
反应条件
sodium methylate; lithium perchlorate; TDBPA in dichloromethane indirect electrochemical oxidation;
参考文献
Tetrahedron, , vol. 42, # 2 p. 553 - 560
反应条件
3,3-dimethyldioxirane in acetone T=25°C; Kinetics;
参考文献
Baumstark; Kovac, Franci; Vasquez, Pedro C.
Heterocyclic Communications, 2002 , vol. 8, # 1 p. 9 - 12
反应条件
CoCl2.6H2O; zinc in tetrahydrofuran T=20°C; 4 h;
参考文献
Sarma, Kuladip; Goswami, Amrit
Letters in Organic Chemistry, 2009 , vol. 6, # 7 p. 568 - 572
反应条件
triethylamine; toluene-4-sulfonic acid in dimethylammonium 2,4-dichlorophenoxyacetate; ethyl acetate
参考文献
BASF Aktiengesellschaft
Patent: US6569355 B1, 2003 ;
反应条件
lithium in tetrahydrofuran T=20°C; 24 h;
参考文献
Azzena, Ugo; Denurra, Teresa; Melloni, Giovanni; Piroddi, Anna Maria
Journal of Organic Chemistry, 1990 , vol. 55, # 20 p. 5532 - 5535
反应条件
1: iodine / dichloromethane / 0 °C 2: silica gel / dichloromethane / 1 h / 20 °C / Molecular sieve View Scheme
参考文献
Villano, Rosaria; Acocella, Maria R.; Scettri, Arrigo
Tetrahedron, 2011 , vol. 67, # 15 p. 2768 - 2772
反应条件
1: dichloromethane / 0.5 h / 0 °C 2: oxygen / dichloromethane / -40 °C View Scheme
参考文献
Goto, Akihiro; Otake, Kazuki; Kubo, Ozora; Sawama, Yoshinari; Maegawa, Tomohiro; Fujioka, Hiromichi
Chemistry - A European Journal, 2012 , vol. 18, # 36 p. 11423 - 11432
参考文献
BASF Aktiengesellschaft
Patent: US5359122 A1, 1994 ;
反应条件
PMES-SO3H-NH2-A T=90°C; Henry reaction; 24 h;
参考文献
Sasidharan, Manickam; Fujita, Satoru; Ohashi, Masataka; Goto, Yasutomo; Nakashima, Kenichi; Inagaki, Shinji
Chemical Communications, 2011 , vol. 47, # 37 p. 10422 - 10424
