甲基(5-甲氧基-2-硝基苯基)乙酸酯合成路线 （共 7 条）
反应条件
chloro-trimethyl-silane T=45°C; 6 h;
参考文献
Cravotto; Giovenzana; Pilati; Sisti; Palmisano
Journal of Organic Chemistry, 2001 , vol. 66, # 25 p. 8447 - 8453
反应条件
amberlyst-15 2 h; Heating;
参考文献
Cravotto; Giovenzana; Pilati; Sisti; Palmisano
Journal of Organic Chemistry, 2001 , vol. 66, # 25 p. 8447 - 8453
反应条件
water in dimethyl sulfoxide RefluxInert atmosphere;
参考文献
Nguyen, Quyen; Nguyen, Tuyen; Driver, Tom G.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 620 - 623
反应条件
sodium hydride T=20 - 60°C;
参考文献
Selvakumar; Azhagan, A.Malar; Srinivas; Krishna, G.Gopi
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9175 - 9178
反应条件
1.1: NaOEt / diethyl ether; ethanol / 3 h / 20 °C 1.2: 67 percent / 30percent H2O2; 2M NaOH / H2O / 1 h / 20 °C / pH 9 2.1: 95 percent / Amberlyst-15 / 2 h / Heating View Scheme
参考文献
Cravotto; Giovenzana; Pilati; Sisti; Palmisano
Journal of Organic Chemistry, 2001 , vol. 66, # 25 p. 8447 - 8453
反应条件
1: 73 percent / NaH / tetrahydrofuran / 20 °C 2: 51 percent / NaH / 20 - 60 °C View Scheme
参考文献
Selvakumar; Azhagan, A.Malar; Srinivas; Krishna, G.Gopi
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9175 - 9178
反应条件
1: sodium hydride / N,N-dimethyl-formamide / 4 h / 0 - 20 °C / |Inert atmosphere 2: water / dimethyl sulfoxide / |Reflux; |Inert atmosphere View Scheme
参考文献
Nguyen, Quyen; Nguyen, Tuyen; Driver, Tom G.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 620 - 623
