2,4-二羟基-3,5-二溴-6-甲基苯甲酸乙酯合成路线 (共 14 条)
反应条件
in acetic acid 1 h; Ambient temperature;
参考文献
Gramatica, Paola; Gianotti, M. Pia; Speranza, Giovanna; Manitto, Paolo
Heterocycles, 1986 , vol. 24, # 3 p. 743 - 750
反应条件
bromine in acetic acid
参考文献
Tetrahedron Letters, , vol. 35, # 44 p. 8171 - 8172
反应条件
diethyl ether; bromine
参考文献
Justus Liebigs Annalen der Chemie, , vol. 117, p. 312
参考文献
Chemische Berichte, , vol. 61, p. 926
反应条件
1: hydrogen; palladium-calcium carbonate; NaOH-solution 2: NaOH-solution / 20 °C View Scheme
参考文献
Sonn
Chemische Berichte, 1928 , vol. 61, p. 926
反应条件
1: palladium; aq. NaOH solution / Hydrogenation 2: aqueous NaOH / 90 °C / kurzes Kochen der angesaeuerten Reaktionsloesung View Scheme
参考文献
Anker; Cook
Journal of the Chemical Society, 1945 , p. 311
反应条件
1: CCl4 / Irradiation 2: aqueous dioxane 3: palladium/calcium carbonate; aq. NaOH solution / Hydrogenation View Scheme
参考文献
Allison; Newbold
Journal of the Chemical Society, 1959 , p. 3335,3340
反应条件
hydrogen; palladium on activated charcoal in sodium hydroxide P=760 Torr; 15 h; Ambient temperature;
参考文献
Gramatica, Paola; Gianotti, M. Pia; Speranza, Giovanna; Manitto, Paolo
Heterocycles, 1986 , vol. 24, # 3 p. 743 - 750
参考文献
Sonn
Chemische Berichte, 1928 , vol. 61, p. 926
反应条件
1: H2, CH3COOH, CH3COONa / Pd/C / 760 Torr / Ambient temperature 2: 81 percent / K2CO3 / acetone / 12 h / Heating 3: 1.) n-butyllithium, diisopropylamine / 1.) THF, -78 deg C, 2.) THF, from -78 deg C to RT View Scheme
参考文献
Bruce, Ian; Spencer, Robert; Tyman, John
Journal of Chemical Research, Miniprint, 1992 , # 7 p. 1773 - 1795