(S)-α-氨基-γ-丁内酯 盐酸盐合成路线 (共 18 条)
反应条件
hydrogenchloride in water 0.25 h;
参考文献
US7368600 B2, ;
Page/Page column 16-17 ;
反应条件
hydrogenchloride; hydrogen; platinum(IV) oxide in methanol; ethanol T=25°C; P=5175.4 Torr; 12 h;
参考文献
Australian Journal of Chemistry, , vol. 38, # 4 p. 621 - 624
反应条件
1: With chloroacetic acid in water; acetic acid; isopropyl alcohol T=50 - 90°C; 7 h; 2: With hydrogenchloride in 1,4-dioxane T=20°C; 3 h; Cooling with ice;
参考文献
Tetrahedron Letters, , vol. 50, # 36 p. 5067 - 5070
反应条件
trifluoroacetic acid in dichloromethane 1.5 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 44, # 2 p. 637 - 642
反应条件
hydrogenchloride in water 1 h; Heating; Yield given;
参考文献
Synthesis, , # 11 p. 1065 - 1067
反应条件
hydrogenchloride in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Acta Chemica Scandinavica, , vol. 44, # 2 p. 189 - 194
反应条件
hydrogenchloride; borane-THF 1.)THF, 0 deg C, 2.)ethanol, 12 h, reflux; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 55, # 15 p. 4763 - 4765
反应条件
hydrogenchloride 3 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synthesis, , # 11 p. 1052 - 1055
反应条件
Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 55, # 15 p. 4763 - 4765
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 44, # 12 p. 2322 - 2325