1,3,5-三苯基-1H-吡唑合成路线 （共 78 条）
反应条件
Bi(NO3)3·5H2O; acetic acid
0.00972222 h; microwave irradiation;
参考文献
Ananthnag, Guddekoppa S.; Adhikari, Adithya; Balakrishna, Maravanji S.
Catalysis Communications, 2014 , vol. 43, p. 240 - 243
反应条件
1: 3,3-bis(ethylthio)-1-phenylprop-2-en-1-one; 3,4,5-trimethoxyphenylboronic acid With tetrakis(triphenylphosphine) palladium(0); caesium carbonate in tetrahydrofuran
T=50°C; Liebeskind-Srogl coupling; 2 h; Inert atmosphere;
2: phenylhydrazine With potassium tert-butylate in tert-butyl alcohol
12 h; Reflux; regioselective reaction;
参考文献
Jin, Weiwei; Yu, Haifeng; Yu, Zhengkun
Tetrahedron Letters, 2011 , vol. 52, # 44 p. 5884 - 5887
反应条件
aluminum oxide
T=20°C; 72 h;
参考文献
Texier-Boullet, F.; Klein, B.; Hamelin, J.
Synthesis, 1986 , # 5 p. 409 - 411
反应条件
potassium tert-butylate in tert-butyl alcohol
9 h; Reflux; regioselective reaction;
参考文献
Jin, Weiwei; Yu, Haifeng; Yu, Zhengkun
Tetrahedron Letters, 2011 , vol. 52, # 44 p. 5884 - 5887
反应条件
thianthrene cation radical perchlorate in acetonitrile
24 h;
参考文献
Kovelesky, Albert C.; Shine, Henry J.
Journal of Organic Chemistry, 1988 , vol. 53, # 9 p. 1973 - 1979
反应条件
1,4-diaza-bicyclo[2.2.2]octane; oxygen; copper diacetate in dimethyl sulfoxide
T=100°C; P=760.051 Torr; 12 h;
参考文献
Li, Xianwei; He, Li; Chen, Huoji; Wu, Wanqing; Jiang, Huanfeng
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3636 - 3646
反应条件
thionyl chloride in pyridine
T=90°C; 8 h;
参考文献
Nishio, Takehiko; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 2149 - 2152
反应条件
hydrogenchloride in ethanol; water
T=20°C; 0.75 h; Ultrasound irradiation;
参考文献
Li, Ji-Tai; Yin, Ying; Li, Ling; Sun, Ming-Xuan
Ultrasonics Sonochemistry, 2010 , vol. 17, # 1 p. 11 - 13
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 20°C; 2 h; Inert atmosphere;
参考文献
Kawai, Hiroyuki; Yuan, Zhe; Tokunaga, Etsuko; Shibata, Norio
Organic Letters, 2012 , vol. 14, # 20 p. 5330 - 5333,4
反应条件
palladium on activated charcoal; K-10 montmorillonite in dichloromethane
T=160°C; 0.5 h; microwave irradiation;
参考文献
Landge, Shainaz M.; Schmidt, Allison; Outerbridge, Verona; Toeroek, Bela
Synlett, 2007 , # 10 p. 1600 - 1604
