2-[(4,4-二甲基-2,6-二氧代环己基)甲基]-5,5-二甲基环己烷-1,3-二酮合成路线 （共 23 条）
反应条件
in methanol; water
T=40 - 45°C; 0.166667 h;
参考文献
Shanmugasundaram, Palanisamy; Prabahar, K. Joseph; Ramakrishnan, Vayalakkavoor T.
Journal of Heterocyclic Chemistry, 1993 , vol. 30, # 4 p. 1003 - 1008
反应条件
in acetonitrile
T=20°C; Condensation; 5 h;
参考文献
Shutalev; Kishko
Chemistry of Heterocyclic Compounds, 2000 , vol. 36, # 1 p. 62 - 64
反应条件
in acetonitrile
Condensation; Heating;
参考文献
Shutalev; Kishko
Chemistry of Heterocyclic Compounds, 2000 , vol. 36, # 1 p. 62 - 64
反应条件
potassium hydroxide; water
T=180°C; 7 h;
参考文献
Bakibaev, A.A.; Filimonov, V.D.; Nevzgodova, E.S.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 7 p. 1332 - 1336
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 7 p. 1519 - 1524
反应条件
1: 23 percent / sodium borohydride / ethanol; various solvent(s); H2O / 2 h / Heating
2: 1.) dichloroethane/methanol, 2 h, 2.) methanol, reflux, 30 min
View Scheme
参考文献
Butler, Anthony R.; Shepherd, Peter T.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 113 - 116
参考文献
Grue-Sorensen, Gunnar; White, Robert L.; Spenser, Ian D.
Journal of the American Chemical Society, 1986 , vol. 108, # 1 p. 146 - 158
反应条件
hydrogenchloride in ethanol; water
参考文献
Desperak, Danuta; Pawlowski, Jacek; Thiel, Jacek
Journal of Molecular Structure, 2004 , vol. 705, # 1-3 p. 167 - 176
参考文献
Ionescu; Bodea
Bulletin de la Societe Chimique de France, 1929 , vol. <4> 45, p. 466
Bulletin de la Societe Chimique de France, 1930 , vol. <4> 47, p. 1415
Full Text Show Details
Ionescu
Bulletin de la Societe Chimique de France, 1928 , vol. <4> 43, p. 677
Full Text Show Details
Ionescu; Georgescu
Bulletin de la Societe Chimique de France, 1927 , vol. <4> 41, p. 705
反应条件
1: 10-bromo-10,11-dihydrocinchonidine With sodium hydrogencarbonate in ethanol; water
18 h; Heating;
2: dimedone With hydrogenchloride in ethanol; water
参考文献
Desperak, Danuta; Pawlowski, Jacek; Thiel, Jacek
Journal of Molecular Structure, 2004 , vol. 705, # 1-3 p. 167 - 176
参考文献
Vorlaender
Fresenius' Zeitschrift fuer Analytische Chemie, 1929 , vol. 77, p. 266
