2,2’-双(1,3-二苯基咪唑啉烯)合成路线 (共 7 条)
反应条件
in 2,4,6-trimethyl-pyridine; xylene T=185°C; 1 h;
参考文献
Duin, Marcel A.; Lutz, Martin; Spek, Anthony L.; Elsevier, Cornelis J.
Journal of Organometallic Chemistry, 2005 , vol. 690, # 24-25 p. 5804 - 5815
反应条件
1: 96 percent / p-toluenesulfonic acid; Na2SO4 / CH2Cl2 / 8 h 2: Thermolysis View Scheme
参考文献
Duin, Marcel A.; Lutz, Martin; Spek, Anthony L.; Elsevier, Cornelis J.
Journal of Organometallic Chemistry, 2005 , vol. 690, # 24-25 p. 5804 - 5815
反应条件
1: 62 percent / Se / 0.5 h / 220 °C 2: 47 percent / 5 h / 150 °C View Scheme
参考文献
Schoenberg, Alexander; Singer, Erich; Stephan, Werner
Chemische Berichte, 1983 , vol. 116, # 6 p. 2068 - 2073
反应条件
sulfur in pyridine 7 h; Heating;
参考文献
Karkhanis, Dattatraya W.; Field, Lamar
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 22, p. 49 - 58
反应条件
air; 9,10-Dibromoanthracene in chloroform
further solvents: dichlorometane, acetonitrile, same reaction without fluorescer;
参考文献
Roeterdink, F.; Scheeren, J. W.; Laarhoven, W. H.
Tetrahedron Letters, 1983 , vol. 24, # 22 p. 2307 - 2310
反应条件
air; 9,10-Dibromoanthracene in chloroform
further solvents: dichlorometane, acetonitrile, same reaction without fluorescer;
参考文献
Roeterdink, F.; Scheeren, J. W.; Laarhoven, W. H.
Tetrahedron Letters, 1983 , vol. 24, # 22 p. 2307 - 2310
反应条件
1: toluene / 1 h / 70 °C
2: 7 percent / benzene / 12 h / Irradiation
View Scheme
参考文献
Regitz, M.; Weise, G.; Lenz, B.; Foerster, U.; Urgast, K.; Maas, G.
Bulletin des Societes Chimiques Belges, 1985 , vol. 94, # 7 p. 499 - 520