反应条件
n-butyllithium in tetrahydrofuran; hexane; toluene N2-atmosphere; dropwise addn. of BuLi (in hexane) to indene derivative (in THF) at -78°C, warming to room temp., stirring for 30 min, dropwise addn. to Zr-complex (in PhMe) over 2 h at 0°C, stirring (room temp., 2 h, pptn.); filtration, washing (THF/PhMe=1:2), drying (vac., overnight); elem. anal.;
参考文献
Lee, Gong Yeal; Xue, Ming; Kang, Myoung Soon; Kwon, Oh Chul; Yoon, Jin-San; Lee, Yoo-Su; Kim, Hoon Sik; Lee, Hyunjoo; Lee, Ik-Mo
Journal of Organometallic Chemistry, 1998 , vol. 558, # 1-2 p. 11 - 18