6,6-二甲基-5-亚甲基-1,3-环戊二烯合成路线 (共 71 条)
反应条件
in benzene 24 h; Heating;
参考文献
Tetrahedron, , vol. 37, p. 1349 - 1357
反应条件
pyrrolidine; acetic acid 1.) MeOH, 0 deg C, 30 min, 2.) room temperature, 1 h; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Synthetic Communications, , vol. 29, # 4 p. 631 - 643
反应条件
in acetone T=20°C; retro-Diels-Alder reaction; Equilibrium constant;
参考文献
Journal of Organic Chemistry, , vol. 68, # 1 p. 120 - 129
反应条件
in deuterated toluene T=20°C; retro-Diels-Alder reaction; Equilibrium constant;
参考文献
Journal of Organic Chemistry, , vol. 68, # 1 p. 120 - 129
反应条件
in benzene-d6 T=76°C; the equilibrium was investigated by 1H-NMR; Product distribution;
参考文献
Helvetica Chimica Acta, , vol. 65, # 1 p. 74 - 88
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 158, p. 1764
Annales de Chimie (Cachan, France), , vol. <9> 4, p. 90,195
反应条件
in benzene Ambient temperature;
参考文献
Tetrahedron, , vol. 37, p. 1349 - 1357
反应条件
ethanol; palladium Hydrogenation;
参考文献
Kasanski; Tatewossjan
Zhurnal Obshchei Khimii, 1939 , vol. 9, p. 2248,2251
Chem. Zentralbl., 1940 , vol. 111, # I p. 3090
Full Text Show Details
Kasanski; Plate; Gnatenko
Chemische Berichte, 1936 , vol. 69, p. 954,957
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 1593,1595
反应条件
T=125°C; P=73550.8 Torr; Hydrogenation;
参考文献
Pines; Ipatieff
Journal of the American Chemical Society, 1939 , vol. 61, p. 1076
反应条件
in diethyl ether 1 h;
参考文献
Keana, John F. W.; Guzikowski, Anthony P.; Morat, Claude; Volwerk, Johannes J.
Journal of Organic Chemistry, 1983 , vol. 48, # 16 p. 2661 - 2666