in tetrahydrofuran Irradiation (UV/VIS); Stirring of nitroso compound in THF under N2, metal carbonyl in THF is added, the soln. is irradiated (sunlamp photolysis) for a period of 1 h.; final purifn. by chromy. on silica gel (dissolving of residue in 19/1 hexane/ethyl acetate);
参考文献
Journal of Organometallic Chemistry, , vol. 368, p. 83 - 102
