1,1,1,2,3-五氯丙烷合成路线 （共 52 条）
反应条件
chlorine
T=0°C; Ultraviolet irradiation;
参考文献
DAIKIN INDUSTRIES, LTD.; NOSE, Masatoshi; SUZUKI, Atsushi; YAMASHITA, Tsuneo; KATSUKAWA, Kenichi
Patent: WO2010/123148 A1, 2010 ;
Location in patent: Page/Page column 11 ;
反应条件
anhydrous iron chloride; chlorine
T=82°C; P=1277.21 Torr; 15.33 h; Product distribution / selectivity;
参考文献
OCCIDENTAL CHEMICAL CORPORATION
Patent: WO2009/85862 A1, 2009 ;
Location in patent: Page/Page column 28 ;
反应条件
copper(l) chloride in acetonitrile
T=150°C; P=12137.6 Torr; 10 h; Product distribution / selectivity;
参考文献
Tung, Hsueh Sung; Shankland, Ian
Patent: US2008/91053 A1, 2008 ;
Location in patent: Page/Page column 4 ;
参考文献
Gerding; Haring
Recueil des Travaux Chimiques des Pays-Bas, 1955 , vol. 74, p. 841,847
Full Text Show Details
Haszeldine
Journal of the Chemical Society, 1953 , p. 3371,3377
反应条件
sulfuryl dichloride; 2,2'-azo-bisisobutyronitrile
T=55 - 60°C;
参考文献
DOW GLOBAL TECHNOLOGIES, LLC; TIRTOWIDJOJO, Max Markus; KRUPER, William J.; FISH, Barry; LAITAR, David Stephen
Patent: WO2012/166394 A1, 2012 ;
Location in patent: Page/Page column 18-19 ;
反应条件
chlorine
T=100°C; Irradiation.mit UV-Licht;
参考文献
Ponomarenko; Snegowa
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2067,2070; engl. Ausg. S. 2122, 2125
Full Text Show Details
Davis; Whaley
Journal of the American Chemical Society, 1951 , vol. 73, p. 2361
反应条件
chlorine in tetrachloromethane
Irradiation;
参考文献
Upton,C.J.; Incremona,J.H.
Journal of Organic Chemistry, 1976 , vol. 41, p. 523 - 530
反应条件
beim Chlorieren; zunaechst im Sonnenlicht in der Dampfphase, dann in fluessiger Phase;
参考文献
Henne; Whaley
Journal of the American Chemical Society, 1942 , vol. 64, p. 1157
参考文献
Freidlina et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1956 , p. 1202,1204;engl.Ausg.S.1229,1231
参考文献
Haszeldine
Journal of the Chemical Society, 1953 , p. 3371,3377
