1,1,1,2,3-五氯丙烷合成路线 （共 52 条）
反应条件
hydrogen fluoride T=290°C; P=750.075 Torr; 3 h; Inert atmospheretubular reactor;
参考文献
Nose, Masatoshi; Yamashita, Tsuneo; Suzuki, Atsushi
Patent: US2012/65434 A1, 2012 ;
Location in patent: Page/Page column 5 ;
反应条件
anhydrous iron chloride T=154 - 157°C; P=350 Torr; 8 h; Conversion of starting material;
参考文献
TOKUYAMA CORPORATION; Hosaka, Shunsuke; Komatsu, Yasutaka; Moriwaki, Masayuki; Yamamoto, Kikuo; Okada, Naoya
Patent: US2013/165705 A1, 2013 ;
Location in patent: Paragraph 0159; 0160 ;
反应条件
T=400°C; P=750.075 Torr; 0.0130556 h; Inert atmosphere;
参考文献
DAIKIN INDUSTRIES, LTD.; NOSE, Masatoshi; SUZUKI, Atsushi
Patent: WO2011/65574 A1, 2011 ;
Location in patent: Page/Page column 12-13 ;
反应条件
hydrogen fluoride T=290°C; 3 h; HASTELLOY.(R). tubular reactorInert atmosphere; Product distribution / selectivity;
参考文献
Nose, Masatoshi; Yamashita, Tsuneo; Suzuki, Atsushi
Patent: US2012/65434 A1, 2012 ;
Location in patent: Page/Page column 5 ;
反应条件
potassium hydroxide T=0°C;
参考文献
Haszeldine
Journal of the Chemical Society, 1953 , p. 3371,3377
反应条件
potassium hydroxide T=0 - 5°C;
参考文献
Haszeldine
Journal of the Chemical Society, 1953 , p. 3371,3377
Full Text Show Details
Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1951 , p. 518,521
Doklady Akademii Nauk SSSR, 1954 , vol. 94, p. 249,252
Chem.Abstr., 1952 , p. 7038,1955 3000
反应条件
hydrogen fluoride; Catalyst M-Chromium oxide T=250 - 400°C; 0.00138889 - 0.0138889 h;
参考文献
HONEYWELL INTERNATIONAL, INC.
Patent: WO2005/108334 A1, 2005 ;
Location in patent: Page/Page column 13-14 ;
反应条件
1: With potassium hydroxide; Aliquatreg; 336 in water
T=80°C; 3 h;
2: With chlorine
T=0°C; 3 h; UV-irradiation;
参考文献
Nose, Masatoshi; Yamashita, Tsuneo; Suzuki, Atsushi
Patent: US2012/65434 A1, 2012 ;
Location in patent: Page/Page column 4 ;
反应条件
chlorine in tetrachloromethane
T=0 - 10°C; 0.00138889 - 0.00555556 h; UV-irradiation;
参考文献
HONEYWELL INTERNATIONAL, INC.
Patent: WO2005/108334 A1, 2005 ;
Location in patent: Page/Page column 13-14 ;
反应条件
AIBMe; chlorine in tetrachloromethane
T=70°C; P=8517.48 Torr; 2.08333 h; Sealed tube; Time;
参考文献
DOW GLOBAL TECHNOLOGIES, LLC; TIRTOWIDJOJO, Max Markus; FISH, Barry; LAITAR, David Stephen
Patent: WO2013/22677 A1, 2013 ;
Location in patent: Page/Page column 0066 ;
