in neat (no solvent) byproducts: mercury, hexaphenylene; finely powdered Bi intimately mixed with (HgC6H4)3 was heated in a sealed tube at 250°C for 2 h; extd. with petroleum ether, ext. was subjected to preparative TLC on SiO2 (petroleum ether-Et2O); products were identified by mass spectrometry;
参考文献
Journal of Organometallic Chemistry, , vol. 319, p. 59 - 68
silica gel; cyclopenta-1,3-diene 1.) 1 h at 900 deg C 2.) CH2Cl2, 2 h at -78 deg C, 18 h at room temp.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Australian Journal of Chemistry, , vol. 48, # 2 p. 185 - 198
