顺式-2,6-二甲基哌嗪合成路线 （共 15 条）
反应条件
hydrogen; cobalt in ammonia T=200°C; P=22502.3 Torr; 3 h;
参考文献
Bayer Aktiengesellschaft
Patent: US6365741 B2, 2002 ;
Location in patent: Example 2 ;
反应条件
ammonia; hydrogen; nickel T=200°C; P=56634.1 Torr;
参考文献
Yuki Gosei Kagaku Kyokaishi, , vol. 17, p. 17,19
Chem.Abstr., , p. 7191
FR1206423 , ;
US2911407 , ;
反应条件
ammonia; hydrogen; nickel T=200°C; P=56634.1 Torr;
参考文献
Yuki Gosei Kagaku Kyokaishi, , vol. 17, p. 131,132, 135
Chem.Abstr., , p. 11392
反应条件
[{(η5-C5Me5)IrCl}2(μ-Cl)2]; sodium hydrogencarbonate in water T=140°C; 17 h; Inert atmosphereHeating; Overall yield = 90percent;
参考文献
European Journal of Organic Chemistry, , # 34 p. 6752 - 6759
反应条件
ammonia; hydrogen; nickel
参考文献
Muehlebach, Andreas; Pino, Piero
Helvetica Chimica Acta, 1990 , vol. 73, # 4 p. 839 - 855
反应条件
potassium hydroxide; nickel monoaluminide 22.8 h;
参考文献
Journal of Organic Chemistry, , vol. 52, # 6 p. 1043 - 1046
反应条件
ammonia bei der Destillation; anschliessend Reduktion;
参考文献
Journal of the Chemical Society, , vol. 101, p. 2331
反应条件
pyridine T=80°C; 0.666667 h;
参考文献
Miyamoto, Teruyuki; Matsumoto, Jun-ichi; Chiba, Katsumi; Egawa, Hiroshi; Shibamori, Koh-ichiro; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 6 p. 1645 - 1656
反应条件
pyridine T=80°C; 0.666667 h;
参考文献
Miyamoto, Teruyuki; Matsumoto, Jun-ichi; Chiba, Katsumi; Egawa, Hiroshi; Shibamori, Koh-ichiro; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 6 p. 1645 - 1656
反应条件
in tetrahydrofuran T=20°C; 4 h;
参考文献
Zhang, Nan; Zhong, Rong
Patent: US2013/116265 A1, 2013 ;
Location in patent: Paragraph 0024; 0025 ;
