2-(dimethylamino)-ethanol; samarium diiodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide 24 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
n-Bu3Sn-AlMe3Li in tetrahydrofuran; hexane T=25°C; 18 h;
参考文献
Matsubara, Seijiro; Nonaka, Tsuyoshi; Okuda, Yasuhiro; Kanemoto, Shigekazu; Oshima, Koichiro; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 5 p. 1480 - 1483
2-(dimethylamino)-ethanol; samarium diiodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide 24 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
