3-环己基-1,1-二甲醇合成路线 (共 6 条)
反应条件
potassium hydroxide in ethanol Heating;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 95, # 3 p. 57 - 66
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 7 h;
参考文献
Organic Letters, , vol. 6, # 24 p. 4411 - 4414
反应条件
1: methanol; Raney nickel / 45 °C / 51485.6 Torr / Hydrogenation 2: PBr3 / 150 °C 3: zinc dust; aqueous ethanol View Scheme
参考文献
Shortridge et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 948
反应条件
1: methanol; Raney nickel / 45 °C / 51485.6 Torr / Hydrogenation 2: PBr3 / 150 °C View Scheme
参考文献
Shortridge et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 948
反应条件
methanol; nickel T=45°C; P=51485.6 Torr; Hydrogenation;
参考文献
French; Gallagher
Journal of the American Chemical Society, 1942 , vol. 64, p. 1497
反应条件
sulfuric acid in dichloromethane
T=20°C; 8 h;
参考文献
Peelen, Timothy J.; Chi, Yonggui; English, Emily Payne; Gellman, Samuel H.
Organic Letters, 2004 , vol. 6, # 24 p. 4411 - 4414