2(4-溴苯甲酰基)苯甲酸合成路线 （共 15 条）
反应条件
1: With AlCl3, aluminium chloride T=90°C; 2 h; 2: With hydrogenchloride in water
参考文献
Golding, Bernard Thomas; Riedinger, Christiane; Griffin, Roger John; Hardcasctle, Ian Robert; Valeur, Eric; Watson, Anna Frances; Noble, Martin
Patent: US2011/224274 A1, 2011 ;
Location in patent: Page/Page column 43 ;
反应条件
palladium (II) trifluoroacetate; silver carbonate in ethylene glycol dimethyl ether T=130°C; 24 h; Sealed tube; chemoselective reaction;
参考文献
Miao, Jinmin; Ge, Haibo
Organic Letters, 2013 , vol. 15, # 12 p. 2930 - 2933
反应条件
anhydrous butyl ether Behandeln des Reaktionsgemisches mit Eis und Schwefelsaeure;
参考文献
Weizmann; Bergmann; Bergmann
Journal of the Chemical Society, 1935 , p. 1367,1368, 1369
参考文献
Allen; Gates
Journal of the American Chemical Society, 1943 , vol. 65, p. 419,421
参考文献
Allen; Gates
Journal of the American Chemical Society, 1943 , vol. 65, p. 419,421
参考文献
Gomberg; Blicke
Journal of the American Chemical Society, 1923 , vol. 45, p. 1775
反应条件
sulfuric acid T=160°C;
参考文献
Heller
Chemische Berichte, 1912 , vol. 45, p. 678
参考文献
Heller
Chemische Berichte, 1912 , vol. 45, p. 678
参考文献
Abouzid, Khaled A. M.; Khalil, Nadia A.; Ahmed, Eman M.
Medicinal Chemistry Research, 2012 , vol. 21, # 10 p. 3288 - 3293,6
Title/Abstract Full Text Show Details
Abouzid, Khaled A.M.; Khalil, Nadia A.; Ahmed, Eman M.
Medicinal Chemistry Research, 2013 , vol. 22, # 3 p. 1057 - 1064
反应条件
1: hydroxyethyl piperidine With sodium hydride in tetrahydrofuran 0.5 h; Reflux; 2: methanol; 2-(4'-bromobenzoyl)benzoic acid With sodium hydride in tetrahydrofuran T=20°C; 3: With thionyl chloride T=0 - 20°C;
参考文献
Miao, Jinmin; Ge, Haibo
Organic Letters, 2013 , vol. 15, # 12 p. 2930 - 2933
