5-氯苯-1,3-二甲酸合成路线 (共 10 条)
反应条件
in potassium permanganate; water
参考文献
Rohm and Haas Company
Patent: US5254584 A1, 1993 ;
参考文献
Rabjohn
Journal of the American Chemical Society, 1948 , vol. 70, p. 3518
参考文献
Bradsher et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1317
反应条件
1: iron-turnings; chlorine / 100 °C 2: aq. NaOH solution View Scheme
参考文献
Rabjohn
Journal of the American Chemical Society, 1948 , vol. 70, p. 3518
反应条件
1: iron; chlorine / 115 - 125 °C 2: aqueous sulfuric acid View Scheme
参考文献
Bradsher et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1317
反应条件
ammonium metavanadate; nitric acid
参考文献
Toda,T.
Bulletin of the Chemical Society of Japan, 1967 , vol. 40, p. 588 - 590
反应条件
potassium hydroxide; potassium permanganate
参考文献
Klages; Knoevenagel
Chemische Berichte, 1895 , vol. 28, p. 2045
反应条件
(i) H2, Pd-C, EtOH, (ii) aq. NaNO2, (iii) CuCl, aq. HCl; Multistep reaction;
参考文献
Toda,T.
Bulletin of the Chemical Society of Japan, 1967 , vol. 40, p. 588 - 590
反应条件
T=130 - 135°C; Einleiten von Phosgen; Behandeln des Reaktionsprodukts mit Wasser;
参考文献
I.G. Farbenind.
Patent: DE745447 , 1940 ;
DRP/DRBP Org.Chem.
参考文献
Rabjohn
Journal of the American Chemical Society, 1948 , vol. 70, p. 3518