1-氯-6,7-二甲氧基异喹啉合成路线 (共 9 条)
反应条件
1: 57 percent / modified Curtius reaction
2: toluene / Heating
3: diphenyl ether / Heating
4: POCl3
View Scheme
参考文献
Tamao, K.; Kodama, S.; Nakajima, I.; Kumada, M.; Minato, A.; Suzuki, K.
Tetrahedron, 1982 , vol. 38, # 22 p. 3347 - 3354
反应条件
1: 60 percent / Perkin reaction
2: 57 percent / modified Curtius reaction
3: toluene / Heating
4: diphenyl ether / Heating
5: POCl3
View Scheme
参考文献
Tamao, K.; Kodama, S.; Nakajima, I.; Kumada, M.; Minato, A.; Suzuki, K.
Tetrahedron, 1982 , vol. 38, # 22 p. 3347 - 3354
反应条件
1: diphenyl ether / Heating
2: POCl3
View Scheme
参考文献
Tamao, K.; Kodama, S.; Nakajima, I.; Kumada, M.; Minato, A.; Suzuki, K.
Tetrahedron, 1982 , vol. 38, # 22 p. 3347 - 3354
反应条件
1: toluene / Heating
2: diphenyl ether / Heating
3: POCl3
View Scheme
参考文献
Tamao, K.; Kodama, S.; Nakajima, I.; Kumada, M.; Minato, A.; Suzuki, K.
Tetrahedron, 1982 , vol. 38, # 22 p. 3347 - 3354
参考文献
Tamao, K.; Kodama, S.; Nakajima, I.; Kumada, M.; Minato, A.; Suzuki, K.
Tetrahedron, 1982 , vol. 38, # 22 p. 3347 - 3354
参考文献
Anderson et al.
Journal of the American Pharmaceutical Association (1912-1977), 1952 , vol. 41, p. 643,648
反应条件
1: palladium/charcoal / 200 - 240 °C / Unter Stickstoff
2: phosphoryl chloride
View Scheme
参考文献
Anderson et al.
Journal of the American Pharmaceutical Association (1912-1977), 1952 , vol. 41, p. 643,648
反应条件
1: phosphoryl chloride; phosphorus (V)-oxide
2: palladium/charcoal / 200 - 240 °C / Unter Stickstoff
3: phosphoryl chloride
View Scheme
参考文献
Anderson et al.
Journal of the American Pharmaceutical Association (1912-1977), 1952 , vol. 41, p. 643,648
反应条件
1: benzene
2: phosphoryl chloride; phosphorus (V)-oxide
3: palladium/charcoal / 200 - 240 °C / Unter Stickstoff
4: phosphoryl chloride
View Scheme
参考文献
Anderson et al.
Journal of the American Pharmaceutical Association (1912-1977), 1952 , vol. 41, p. 643,648