反应条件
in tetrahydrofuran addn. of soln. of bromostyrene to suspn. of Mg, refluxing (2 h), coolingto 195 K, dropwise addn. of borate ( 2 h), warming to ambient temp. (ov ernignt); diln. (ether), washing (HCl, H2O, KOH soln.), acidification, extn. (ether), drying of ether phase (over MgSO4), concn., recrystn. (H2O); detd. by (1)H and (13)C NMR spectroscopy;
参考文献
Gainsford, Graeme J.; Meinhold, Richard H.; Woolhouse, Anthony D.
Acta Crystallographica, Section C: Crystal Structure Communications, 1995 , vol. 51, # 12 p. 2694 - 2696
