2-(4-溴苯基)-5-苯基-1,3,4-恶二唑合成路线 (共 19 条)
反应条件
1: With sodium hydrogencarbonate in tetrahydrofuran; water T=20°C; 2: With trichlorophosphate in toluene Reflux;
参考文献
Advanced Functional Materials, , vol. 20, # 18 p. 3012 - 3024
参考文献
Koldobskii, G. I.; Ivanova, S. E.
Russian Journal of General Chemistry, 1994 , vol. 64, # 10.2 p. 1512 - 1517
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 10 p. 1698 - 1704
反应条件
1: pyridine 2: POCl3 View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 29, p. 3054,3055; engl. Ausg. S. 3020, 3021
反应条件
1: aq. NaHCO3 / tetrahydrofuran / 0.5 h 2: 90 percent / POCl3 / 6 h / Heating View Scheme
参考文献
Journal of Physical Chemistry B, , vol. 105, # 37 p. 8845 - 8860
反应条件
1: pyridine / Heating 2: trichlorophosphate / 10 h / Reflux View Scheme
参考文献
Magnetic Resonance in Chemistry, , vol. 49, # 10 p. 648 - 654
反应条件
1: triethylamine 2: trichlorophosphate / 5 h / Reflux; Inert atmosphere View Scheme
参考文献
Inorganica Chimica Acta, , vol. 391, p. 50 - 57
参考文献
Journal of Heterocyclic Chemistry, , vol. 14, p. 1089 - 1092
反应条件
1: hydrazine 2: pyridine / Heating 3: trichlorophosphate / 10 h / Reflux View Scheme
参考文献
Magnetic Resonance in Chemistry, , vol. 49, # 10 p. 648 - 654
反应条件
1.1: n-butyllithium / hexane / 2 h / -5 °C / Inert atmosphere
1.2: 2.75 h / -50 - 20 °C / Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene / 24 h / 110 °C / Inert atmosphere
View Scheme
参考文献
Xu, Qiu-Lei; Li, Hong-Yan; Wang, Cheng-Cheng; Zhang, Song; Li, Tian-Yi; Jing, Yi-Ming; Zheng, You-Xuan; Huang, Wei; Zuo, Jing-Lin; You, Xiao-Zeng
Inorganica Chimica Acta, 2012 , vol. 391, p. 50 - 57