3,4-二羟基苯甲酸甲酯合成路线 (共 60 条)
反应条件
thionyl chloride Heating;
参考文献
Pandey, Rajesh K.; Jarvis, Gregory G.; Low, Philip S.
Tetrahedron Letters, 2012 , vol. 53, # 13 p. 1627 - 1629
反应条件
toluene-4-sulfonic acid in methanol 120 h; Heating;
参考文献
Fresco, Zachary M.; Suez, Itai; Backer, Scott A.; Frechet, Jean M. J.
Journal of the American Chemical Society, 2004 , vol. 126, # 27 p. 8374 - 8375
反应条件
1: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in water; carbonic acid dimethyl ester T=20°C; 2: With anhydrous sodium oxalate in water; carbonic acid dimethyl ester chemoselective reaction;
参考文献
Bernini, Roberta; Barontini, Maurizio; Mosesso, Pasquale; Pepe, Gaetano; Willfoer, Stefan M.; Sjoeholm, Rainer E.; Eklund, Patrik C.; Saladino, Raffaele
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 11 p. 2367 - 2377
反应条件
sodium dithionite; sodium bis(2-ethylhexyl)-sulfosuccinate; oxygen; Flavin mononucleotide in 2,2,4-trimethylpentane Ambient temperature; Product distributionMechanism;
参考文献
Chauhan, S. M. S.; Awasthi, Abha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 10 p. 872 - 875
反应条件
hydrogenchloride in diethyl ether T=20°C; 0.0166667 h;
参考文献
Carato, Pascal; Laconde, Guillaume; Ladjel, Chehla; Depreux, Patrick; Henichart, Jean-Pierre
Tetrahedron Letters, 2002 , vol. 43, # 37 p. 6533 - 6535
反应条件
(N,N-[2-(2-Py)Et]2-α,α-D2-benzyl-amine)2(peroxo)Cu2(PF6)2 in methanol; acetone 0.25 h;
参考文献
Itoh; Kumei; Taki; Nagatomo; Kitagawa; Fukuzumi
Journal of the American Chemical Society, 2001 , vol. 123, # 27 p. 6708 - 6709
反应条件
thionyl chloride in methanol
反应条件
toluene-4-sulfonic acid in methanol; diethyl ether
反应条件
aluminum tri-bromide in ethanethiol T=0°C; 1 h;
参考文献
Node, Manabu; Nishide, Kiyoharu; Fuji, Kaoru; Fujita, Eiichi
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4275 - 4277
反应条件
α,α'-bislt;bislt;2-(1'-methyl-2'-benzimidazolyl)ethylgt;aminogt;m-xylene - Cu(MeCN)4ClO4 (1:2 complex); oxygen in acetonitrile
参考文献
Casella, Luigi; Gullotti, Michele; Radaelli, Roberto; Gennaro, Patrizia Di
Journal of the Chemical Society, Chemical Communications, 1991 , # 22 p. 1611 - 1612