2-(二甲基氨基)-1-[(二甲基氨基)甲基]乙基甲基丙烯酸酯合成路线 （共 2 条）
反应条件
1: methacrylic acid methyl ester With (10H)-phenothiazine; tris(nonylphenyl)phosphite; 1,4-dimethoxy benzene T=96°C; P=760.051 Torr; Heating / reflux; 2: With oxygen; lithium oxide T=121°C; 1.66667 h; 3: N,N,N',N'-tetramethyl-2-hydroxy-1,3-propanediamine T=107 - 112°C; 5 - 6 h; Product distribution / selectivity;
参考文献
Taminco N.V.
Patent: EP1512676 A1, 2005 ;
Location in patent: Page/Page column 7-8 ;
反应条件
(10H)-phenothiazine; sodium methylate in methanol
参考文献
Korshunov,M.A. et al.
Zhurnal Organicheskoi Khimii, 1969 , vol. 5, # 11 p. 1947 - 1952,1893 - 1898
