反应条件
hydrogenchloride in diethyl ether under N2; to cold (-98 °C) soln. of boron compd. in Et2O slowly added Cl2HCLi, stirred for 1 h, warmed to room temp., stirred for 3 h, cooled to 0 °C, added soln. of anhyd. HCl in Et2O, stirred for 0.5 h; decanted and combined with ether washes of solid, evapd. in air, distd.; elem. anal.;
参考文献
Brown, Herbert C.; Cole, Thomas E.
Organometallics, 1983 , vol. 2, p. 1316 - 1319
