5,6-二氢-5-三氟甲基尿嘧啶合成路线 （共 6 条）
反应条件
triethylamine; PdCl2(PPh3) in N,N-dimethyl-formamide T=60°C; P=34200 Torr; 18 h;
参考文献
Fuchikami, Takamasa; Ojima, Iwao
Tetrahedron Letters, 1982 , vol. 23, # 40 p. 4099 - 4100
反应条件
acetic anhydride; urea
反应条件
in acetic anhydride T=100°C; 1 h;
参考文献
Fuchikami; Yamanouchi; Ojima
Synthesis, 1984 , vol. NO. 9, p. 766 - 768
反应条件
sulfuric acid; iodine in water; dimethyl sulfoxide
参考文献
MITSUI TOATSU CHEMICALS, Inc.
Patent: EP635517 A1, 1995 ;
反应条件
copper(ll) bromide in acetic acid; N,N-dimethyl-formamide T=115°C; 14 h; var. temp. time and solv.: aq. DMF; constant-electrolysis with Pt electrodes with KBr;
参考文献
Fuchikami, Takamasa; Yamanouchi, Akiko
Chemistry Letters, 1984 , p. 1595 - 1598
反应条件
potassium bromide in water; N,N-dimethyl-formamide constant-current electrolysis with Pt electrodes; var. reag.: CuBr2;
参考文献
Chemistry Letters, , p. 1595 - 1598
